Crystal structure of (5,14-methyl-7,12-dimethyl-1,4,8,11-tetraazadiiminecyclotetradecylene-N,N',N'',N''')nickel(II) bis(diisopropyldithiophosphate) complex.

نویسندگان

  • Fangfang Jian
  • Kui Jiao
  • Faqian Liu
  • Qingxiang Wang
چکیده

The macrocyclic tetradentate Ni(II) compound was obtained in a reaction and determined by X-ray diffraction. The crystal structure shows that the molecule is centrosymmetric, and Ni atom located in a square planar coordination environment. The two [(iPrO)2PS2]- anions are outside the macrocycle complex to balance. The Ni-N bond lengths are in the range of 1.906(2) to 1.950(2)A.

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عنوان ژورنال:
  • Analytical sciences : the international journal of the Japan Society for Analytical Chemistry

دوره 19 4  شماره 

صفحات  -

تاریخ انتشار 2003